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- W2371567425 abstract "Objective To develop and validate a specific,sensitive and rapid method for the determination of multi-residual non-steroidal anti-inflammatory drugs(NSAIDs)(ketoprofen,meloxicam,diclofenac,ibuprofen)in aquatic environment by SPE-HPLC.Method The sample pretreatment was operated by solid phase extraction(SPE).The determination was performed on a C18 co-lumn(200 mm × 4.6 mm,5 μm),the mobile phase included acetonitrile and 20 mmol·L-1 ammonium acetate in water,adjusted to pH 3.5 by addition of acetic acid,the flow rate was 1.0 mL· min-1 and wavelength was set at 263 nm.Results The linear calibration curves were obtained over the concentration range of 0.5-50.0 mg·L-1.Quantification limit of the method was 0.5 mg·L-1.The range of precision was 0.6%-2.0 %.The method extraction recoveries were higher than 78.0%,and sample solutions were stable within 12 h.Conclusion The method was simple,sensitive,accurate and reliable for determination of NSAIDs in aquatic environment." @default.
- W2371567425 created "2016-06-24" @default.
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- W2371567425 date "2010-01-01" @default.
- W2371567425 modified "2023-09-26" @default.
- W2371567425 title "Determination of non-steroidal anti-inflammatory drugs in aquatic environment by SPE-HPLC" @default.
- W2371567425 hasPublicationYear "2010" @default.
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