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- W2371796766 abstract "Objective To develop an RP-HPLC method for simultaneous determination of gallic acid,5hydroxylmethyl furfural,morroniside,loganin,sweroside,paeonol and paeoniflorin in Liuwei Dihuang(traditional Chinese medicine)osmotic pump-controlled release tablets.Methods Isolation of sample was achieved on a Diamonsil C18column(250 mm×4.6 mm,5μm).The column temperature was maintained at 35℃and detection wavelength was set at 254 nm.Solvent A(water,0.06%phosphoric acid,V∶V)and solvent B(acetonitrile,0.06%phosphoric acid,V∶V)were used for gradient elution.The flow rate was 1.0 mL·min-1.Results The linearity ranges of gallic acid,5-hydroxylmethyl furfural,morroniside,loganin,sweroside,paeonol and paeoniflorin were 3.992-19.96 mg·L-1,8.710-43.55 mg· L-1,5.613-28.06 mg·L-1,8.772-43.86 mg·L-1,0.721 7-3.608 mg·L-1,1.643-8.215 mg·L-1 and 14.60-73.00 mg·L-1,respectively(r≥0.999 7).The average recoveries(n=9)of them were 96.1%,100.5%,99.1%,101.1%,102.6%,97.8% and 102.5%,respectively.Conclusions The method is simple,rapid and accurate.It can be applied for the quality control of Liuwei Dihuang osmotic pump-controlled release tablets." @default.
- W2371796766 created "2016-06-24" @default.
- W2371796766 creator A5078562482 @default.
- W2371796766 date "2013-01-01" @default.
- W2371796766 modified "2023-09-27" @default.
- W2371796766 title "Simultaneous determination of gallic acid,5-hydroxylmethyl furfural,morroniside,loganin,sweroside, paeonol and paeoniflorin in Liuwei Dihuang osmotic pump-controlled release tablets by HPLC" @default.
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