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- W2371866874 abstract "Tetraacetyldinitrohexaazaisowurtzitane (TADN),an intermediate in the preparation of CL-20,has been synthesized readily via the nitration of tetraacetylhexaazaisowurtzitane with HNO3/AC2O mixture. The TADN′s structure was determined by X-ray diffraction technique. Its crystal belongs to monoclinic,system and has space group P21/n with parameters: a=1.12231(8) nm,b=1.41083(10) nm,(c=1.12331(8) nm),Z=4,V=1.7395(2) nm~3,dc=1.628 g·cm~(-3),β=102.039(2)°. The length of (C(5)-C(6)) bond is 0.1586 nm,a bit longer than that of normal sp~3 C-C bond and shorter than the corresponding bond in CL-20. This is due to the fact that,in comparison with CL-20,the electron withdrawing effects of acetyl groups positioned in the two five-membered rings of TADN are weaker." @default.
- W2371866874 created "2016-06-24" @default.
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- W2371866874 date "2004-01-01" @default.
- W2371866874 modified "2023-09-23" @default.
- W2371866874 title "Synthesis and Characterization of Tetraacetyldinitrohexaazaisowurtzitane" @default.
- W2371866874 hasPublicationYear "2004" @default.
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