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- W2372088257 abstract "In order to understand the influence of FOX-7 crystal shape and size on its thermal properties,the FOX-7 crystal was obtained from system DMF/H2O and NMP/H2O by cooling crystallization and the antisolvent crystallization.SEM results show that the obtained crystal have two shapes,namely extended tetrahedral or hexahedral prism and rhombohedral prismatic crystal.The size and contained number of particles of the crystal from different ratio system are different.The crystals shape by ultrasonic treatment was single,but the crystals surface is comparatively rough.DSC results show that the thermal properties of FOX-7 obtained by different ways and different solvent system have a certain degree of difference.This indicates that FOX7 crystal with different shapes,sizes and thermal properties can be obtained by the crystallization in different ways and solvent system.The crystals shape was controlled by ultrasonic treatment." @default.
- W2372088257 created "2016-06-24" @default.
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- W2372088257 date "2009-01-01" @default.
- W2372088257 modified "2023-09-26" @default.
- W2372088257 title "Preparation and Thermal Properties of FOX-7" @default.
- W2372088257 hasPublicationYear "2009" @default.
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