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- W2372181698 abstract "It was founded that ampicillin could react with hydrogen peroxide generating chemiluminescence(CL),surfactant cetyltrimethyl ammonium bromide can enhance the CL intensity. The kinetics of CL showed that the CL process was a 200 s tardily process and a slow process which could maintain a number of hours. Through the fluorescence spectra,UV spectra,chemiluminescence spectrum and other test results,it was found that the reaction of hydrogen peroxide and ampicillin was slow reaction,surfactant just could enhance the luminescence intensity,could not catalyze the reaction. In absence of surfactant,Fe( II) ions can accelerate and catalyze the reaction of ampicillin and hydrogen peroxide. Based on this,a new CL method to detect ampicillin was developed. Under the optimized conditions,the first CL peak intensity was linearly with the concentration of ampicillin in the range from 1. 0 × 10- 6g / mL to 2. 5 × 10- 4g / mL with the relative standard deviations within 2. 3%( n = 7),and the detection limit was 4 × 10- 7g / mL. The slow light features provide a reference for establishing chemiluminescence time-resolved detection method. Fe( II) ions can catalyze the reaction of ampicillin with hydrogen peroxide. CL mechanism was also discussed preliminary The slow light features of this CL reaction provided a reference for establishing CL time-resolved detection method." @default.
- W2372181698 created "2016-06-24" @default.
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- W2372181698 date "2013-01-01" @default.
- W2372181698 modified "2023-09-25" @default.
- W2372181698 title "Chemiluminescence behaviors of ampicillin and its analytical determination" @default.
- W2372181698 hasPublicationYear "2013" @default.
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