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- W2372188419 abstract "A copper(I) coordination polymer,[Cu_(3)(etu)_(3)Br_(3)]_(n)(etu = ethylenethiourea),was synthesized by a reaction of CuBr_(2)with etu.It crystallizes in triclinic crystal system,space group Pī,with a= 0.762 46(6) nm,b= 1.198 48(10) nm,c= 1.224 52(7) nm,α = 68.202(5)°,β= 74.607(6)°,γ = 87.652(7)°,V = 0.999 61(13) nm~(3),Z= 2,M_(r)= 736.82,D_(c)=(2.448 )g·cm~(-3),μ=(9.477 mm~(-1)),F(000) = 708,R_(1)= 0.030 6,wR_(2)= 0.071 0.The crystal structure consists of self-assembled Cu_(4)S_(2)Br_(2) and Cu_(2)Br_(2) cores,which are alternately linked by two μ_(2)-S bridges to form [Cu_(3)(μ_(3)-etu)(μ_(2)-etu)_(2)(μ_(2)-Br)_(2)Br]_(n) polymeric chains paralleling b axis.The three crystallographically independent copper(I) ions are in distorted tetrahedral coordination geometry.The etu ligands coordinated to Cu(I) through S atom with the coordination modes of μ_(2)-S and μ_(3)-S." @default.
- W2372188419 created "2016-06-24" @default.
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- W2372188419 date "2006-01-01" @default.
- W2372188419 modified "2023-09-26" @default.
- W2372188419 title "Synthesis and Crystal Structure of Coordination Polymer [Cu_(3)(etu)_(3)Br_(3)]_(n)" @default.
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