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- W2372227584 abstract "A simple flow injection chemiluminescence procedure for the determination of andrographolide was proposed,which is based on the CL emitting reaction between andrographolide and potassium permanganate in acidic medium,greatly enhanced by formaldehyde.Cetyl trimethyl ammonium bromide can further enhance the CL signal of the system.Under the optimized experimental conditions,andrographolide could be determined in a linear range from 5.0 × 10-6 to 2.5 × 10-4 g·mL-1 with a detection limit of 1.0 × 10-6 g·mL-1.The relative standard deviation of the proposed method calculated from 12 repetitive injections of 1.0 × 10-5 g·mL-1 andrographolide was 0.9%.The sample throughput was 150 h-1.The proposed method has been satisfactorily applied to the determination of andrographolide in pharmaceutical formulations with no evidence of interference from common medicaments.In addition,the CL reaction mechanism of KMnO4-HCHO-AD system was also explored.The proposed method provided a strategy for rapid determination of andrographolide." @default.
- W2372227584 created "2016-06-24" @default.
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- W2372227584 date "2010-01-01" @default.
- W2372227584 modified "2023-09-22" @default.
- W2372227584 title "Flow Injection Chemiluminescence Determination of Andrographolide Using Potassium Permanganate and Formaldehyde System" @default.
- W2372227584 hasPublicationYear "2010" @default.
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