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- W2372244220 abstract "Objective:To establish a quality control method for identification and assay of ilexsaponin A for Aikeqing Capsules,a compound Chinese materia medica Radix Ilicis Pubescentis containing.Method: Ilexsaponin A was isolated and identified from the roots of Ilex pubescens.The Phenomenex Kromasil C18(4.6 mm×250 mm,5 μm) column with a Phenomenex Security Guard C18 guard column was used with methanol-0.2% acetic acid(67∶33) as the mobile phase at a flow rate of 1.0 mL·min-1.The drift tube temperature of ELSD was set at 95 ℃,the gas flow was at 2.5 L·min-1.Result: Ilexsaponin A was identified by silica gel TLC from the compound preparation of Chinese materia medica.The linear range of ilexsaponin A was 1.92-9.60 μg(r=0.999 5),and its average recovery was 99.85% with RSD 1.04%.Conclusion: The methods established are rapid and accurate,and can be used for quality control on Radix Ilicis Pubescentis or its compound preparation." @default.
- W2372244220 created "2016-06-24" @default.
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- W2372244220 date "2011-01-01" @default.
- W2372244220 modified "2023-09-28" @default.
- W2372244220 title "HPLC-ELSD Determination of Ilexsaponin A in Aikeqing Capsules" @default.
- W2372244220 hasPublicationYear "2011" @default.
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