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- W2372413488 abstract "The effects of pulse potential,discharging times,Ni2+ concentration,pH value and rare earth additives(LaCl3,NdCl3)on the conversion ratio of Ni2+ as well as the structure,shape and average diameter of Ni-P nanopowders prepared by pulse discharging in solution were investigated by X-ray diffraction(XRD),field emission scanning electron microscopy(FESEM),and focused beam reflectance measurement(FBRM).It is indicated that discharging energy is the key factor that influences the size of Ni-P nanopowders and the conversion ratio of Ni2+.With the increasing of pulse potential or discharging times,the average diameter of Ni-P nanopowders decreased while the conversion ratio of Ni2+ increased.The real-time monitoring results of FBRM showed that the velocities of nucleating and growing of Ni-P particles during the course of discharging were remarkably higher than those after discharging.The size of Ni-P nanopowders could be reduced by adding LaCl3 or NdCl3 to precursor solution.The average diameters of Ni-P nanopowders were 156 nm at the LaCl3 concentration of 0.1 g·L-1 and 72 nm at the NdCl3 concentration of 0.05 g·L-1,respectively." @default.
- W2372413488 created "2016-06-24" @default.
- W2372413488 creator A5022170089 @default.
- W2372413488 date "2010-01-01" @default.
- W2372413488 modified "2023-10-08" @default.
- W2372413488 title "Synthesis of Ni-P nanopowders via pulse discharging in aqueous solution" @default.
- W2372413488 hasPublicationYear "2010" @default.
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