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- W2372728150 abstract "The title compound was synthesized by the reaction of TPA·3HClO 4 with FeCl 3·6H 2O in methanol. Formula C 36 H 36 Cl 4Fe 2N 8O 9, M r =978.22. The X ray crystal structure analysis shows that the crystal is monoclinic, space group C2/c, with a=16.3003(3), b=17 180(3), c=16 582(3), V=4313 3, Z=4, D c =1.299g/cm 3, the final R=0.043, R w =0.049 for 4211 observable reflections. X ray crystallographic studies indicated the presence of a single bridged diiron core in the title compound. The Fe-O-Fe bond angle is 174.4°, while the Fe…Fe distance is 3.565. The iron(Ⅲ) is six coordinated by four nitrogen atoms from TPA, one chloride ion and one μ oxo atom, with a distorted octahedral coordination environment." @default.
- W2372728150 created "2016-06-24" @default.
- W2372728150 creator A5033120372 @default.
- W2372728150 date "1999-01-01" @default.
- W2372728150 modified "2023-09-28" @default.
- W2372728150 title "Synthesis and Crystal Structure of Oxo Bridge Binuclear Iron(III) Complex 〔Fe_2( μ-O)(TPA)_2Cl_2〕(ClO_ 4)_2" @default.
- W2372728150 hasPublicationYear "1999" @default.
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