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- W2373063948 abstract "OBJECTIVE: To establish a method for the content determination of Cefoselis sulfate for injection. METHODS: HPLC method was adopted. The separation was performed on Ultimate C18 column and the column temperature was 30 ℃. The mobile phase consisted of methanol-water (20 ∶ 80) with a flow rate at 1 mL·min-1. The detection wavelength was set at 257 nm and injection volume was 20 μL. RESULTS: The linear range of cefoselis sulfate was 10.0～120.0 μg·mL-1 (r=0.999 9). The detection limit was 0.01 μg·mL-1. The method recoveries were 101.9%, 100.3% and 99.5% at low, medium, high concentrations. The intra-day RSD were 1.07%, 1.38% and 1.40%, and inter-day RSD were 1.07%, 2.58% and 2.87%, respectively. The average content of 3 batches of Cefoselis sulfate for injection was (96.5±1.7)%. CONCLUSION: The method is simple and sensitive for the content determination of Cefoselis sulfate for injection." @default.
- W2373063948 created "2016-06-24" @default.
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- W2373063948 date "2011-01-01" @default.
- W2373063948 modified "2023-09-23" @default.
- W2373063948 title "Content Determination of Cefoselis Sulfate for Injection by HPLC" @default.
- W2373063948 hasPublicationYear "2011" @default.
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