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- W2373112419 abstract "Two Pd/Al2O3 catalysts were synthesized by using K2[PdCl4] and a mixture of K2[PdCl4] and oxalic acid as precursors,respectively. The samples were characterized by means of inductively coupled plasma atomic emission spectroscopy (ICP-AES),transmission electron microscopy (TEM) and temperature-programmed reduction (TPR). The catalytic activities of the samples were tested in the transformation of α-cumyl alcohol (CA) from cumene hydroperoxide (CHP) in cumene solution with hydrogen as a reducing agent in a fixed bed reactor. The results showed that the Pd particles loading on the alumina were misdistribution and agglomeration with a mean particle diameter of about 5-10 nm,and Pd-Al alloy was formed in the treatments of calcinations and reduction due to the strong interaction between Pd and Al2O3. The CHP conversion of 100% and the mean CA selectivity of 97.7% were obtained,respectively,in 240 h CHP hydrogenation over Pd/Al2O3 prepared from K2[PdCl4]. Meanwhile,reaction pathways of catalytic hydrogenation of CHP in cumene solution over Pd/Al2O3 were also discussed on the basic of analyzing and comparing the compositions of the system before and after reaction." @default.
- W2373112419 created "2016-06-24" @default.
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- W2373112419 date "2009-01-01" @default.
- W2373112419 modified "2023-09-26" @default.
- W2373112419 title "CATALYTIC HYDROGENATION OF CUMENE HYDROPEROXIDE OVER Pd/Al_2O_3 CATALYST" @default.
- W2373112419 hasPublicationYear "2009" @default.
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