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- W2373485148 abstract "Objective To establish a gradient elution HPLC method for determining three constituents of Gaoyuankang capsules:aminophylline,dexamethasone sodium phosphate and diazepam.Methods Athena C18-WP(5 μm,100 4.6 mm × 250 mm Serial No.0AG72U42) column was used.The mobile phase consisted of 0.05 mol/L sodium dihydrogen phosphate solution as mobile phase A and methanol as mobile phase B.Gradient elution was used.The detection wavelength was 240 nm and the flow rate was 1.0 ml/min.Results The linear response ranged from 400.03 to 2800.2 μg/ml for aminophylline(r=0.9999),5.998 to 20.993 μg/ml for dexamethasone sodium phosphate(r=0.9999),and 10.008 to 75.06 μg/ml for diazepam(r=0.9999).The mean recovery of aminophylline,dexamethasone sodium phosphate and diazepam was 99.58%,99.97%,99.74%,respectively.Conclusion This method is quick and simple,which may be used for the simultaneous determination of the three constituents in Gaoyuankang capsules." @default.
- W2373485148 created "2016-06-24" @default.
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- W2373485148 date "2012-01-01" @default.
- W2373485148 modified "2023-09-24" @default.
- W2373485148 title "Simultaneous Determination of Aminophylline Dexamethasone Sodium Phosphate and Diazepam in Gaoyuankang Capsules by Gradient Elution HPLC Method" @default.
- W2373485148 hasPublicationYear "2012" @default.
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