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- W2373563231 abstract "A method for simultaneous determination of 4 tetracyclines and 3 epimers in honey samples was developed by high performance liquid chromatography coupled with tandem mass spectrometry.The residues in honey samples were extracted by EDTA-Mcllvaine buffer,and cleaned up and condensed by OASIS hydrophilic-liphophilic balance(HLB) column and weak cation exchange(WCX and carboxylic acid) sequentially.Sample solution eluted from the WCX SPE column by mobile phase was filtered by micro-pours membrane,separated by LC-MS/MS with gradient elution using acetonitrile-formic acid solution as mobile phase and then qualitatively and quantitatively analyzed by ESI-MS/MS in a MRM mode.Baseline separation of 7 target drugs was achieved within 7 min,and qualitative and quantitative analysis was completed.The recovery rates of the spiked samples at trace levels were in the range of 64.9% to 91.0% with the relative standard deviation(RSD) less than 10.5%(n = 7).The detection limits were 1μg/kg for oxytetracycline,tetracyclines,4-epitetracycline,4-epioxytetracycline and 2 μg/kg for chlortetracycline,doxycycline and epichlortetracycline.The developed method was sensitive and reliable,and can be successfully applied to the simultaneous detection of 7 target tetracyclines residues including toxic metabolites in honey." @default.
- W2373563231 created "2016-06-24" @default.
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- W2373563231 date "2011-01-01" @default.
- W2373563231 modified "2023-09-23" @default.
- W2373563231 title "Simultaneous Determination of 4 Tetracyclines and 3 Epimers in Honey by HPLC Coupled with Tandem MS" @default.
- W2373563231 hasPublicationYear "2011" @default.
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