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- W2373866829 abstract "A simultaneous determination of synephrine,hesperidin,naringenin and naringin in Fructus anrantii Immaturus and Fructus aurantii by capillary electrophoresis with electrochemical detection(CE-ED) was reported.Effects of several important factors such as the pH and running buffer concentration,separation voltage,injection time,and detection potential were investigated to acquire the optimum conditions.Under the optimum conditions,the analytes could be separated within 20 min in a 75 cm length capillary at a separation voltage of 12 kV in a 80 mmol·L-1 borate buffer(pH 8.45).A 300 μm diameter carbon disk electrode generates good response at +0.85 V(vs.SCE) for all analytes.The relationship between peak currents and analyte concentrations was linear over about three orders of magnitude with detection limits(S/N=3) ranging from 2×10-4-5×10-4 g·L-1 for all analytes.This proposed method demonstrated long-term stability and reproducibility with relative standard deviations of less than 4% for both migration time and peak current(n=7).It has been successively used for the determination of these analytes in real samples,and the assay result was satisfactory." @default.
- W2373866829 created "2016-06-24" @default.
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- W2373866829 date "2007-01-01" @default.
- W2373866829 modified "2023-09-28" @default.
- W2373866829 title "Determination of Flavonoids in Fructus Anrantii Immaturus and Fructus Aurantii by Capillary Electrophoresis with Electrochemical Detection" @default.
- W2373866829 hasPublicationYear "2007" @default.
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