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- W2373886146 abstract "Objective To establish an HPLC fingerprint of Qingdu Anshen capsules.Methods The fingerprint was obtained on an Ultimate XB-C18 column(3.0 mm×150 mm,3 μm) with the solvent system composed of acetonitrile(A)-0.04% phosphoric acid(B).The elution profile(nonlinear gradient) was: 0-10 min(2%→18%A),10-20 min(18%A),20-55 min(18%→30%A),and 55-90 min(30%→88%A).The detective wavelengths were 203 nm and 260 nm.The column temperature was 30 ℃and the flow rate was 0.6 mL·min-1.Results In the established fingerprint,34 common chromategraphic peaks covering 9 medicinal materials were detected,and 20 chemical compounds were identified by RRLC/MS/MS and PDA spectra.Conclusion The method can be used for the quality control of Qingdu Anshen capsules with great precision and good reproducibility." @default.
- W2373886146 created "2016-06-24" @default.
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- W2373886146 date "2012-01-01" @default.
- W2373886146 modified "2023-09-23" @default.
- W2373886146 title "HPLC fingerprint of Qingdu Anshen capsules" @default.
- W2373886146 hasPublicationYear "2012" @default.
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