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- W2374156454 abstract "A new process for catalytic synthesis of decabromodiphenylethane was developed by brominating diphenylethane with bromine chloride and bromine solution to decrease bromine consumption and simplify post-treatment process.The brominating reagent was prepared by conducting chlorine into bromine at-5℃~0℃.Diphenylethane chloroform solution was dripped into obtained brominating reagent in the presence of aluminum trichloride catalyst at 0℃~5℃.Under the conditions of molar ratio of bromine chloride to diphenylethane and bromine to diphenylethane are 10 ∶1,15 ∶1 respectively,and reaction time is 5 h,decabromodiphenylethane yield and average bromination number are 98.4% and 9.8 respectively.The bromine content and chlorine content of sample are 81.0% and 0.9% respectively." @default.
- W2374156454 created "2016-06-24" @default.
- W2374156454 creator A5059363542 @default.
- W2374156454 date "2008-01-01" @default.
- W2374156454 modified "2023-09-27" @default.
- W2374156454 title "Catalytic Synthesis of Decabromodiphenylethane with Bromine Chloride and Bromine" @default.
- W2374156454 hasPublicationYear "2008" @default.
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