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- W2374285163 abstract "OBJECTIVES To establish a reversed phase high performance liquid chromatographic method with pre-column ultraviolet derivatization for the determination of perfluorooctanoic acids (PFOA) in sewage and urine. METHODS PFOA in sewage and urine formed an ion-pair with tetrabutylammonium (TBA) and were extracted into MTBE. The PFOA then reacted with omega-bromoacetophenone (omega-BAP) in acetonitrile and produced materials quantifiable by HPLC with UV detector. RESULTS The detection limit of the proposed method was 7.0 microg/L with a relative standard deviation of less than 10%. The recoveries for real samples ranged from 85.3% to 116%. CONCLUSION The proposed method is suitable for the determination of PFOA in sewage and urine." @default.
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- W2374285163 date "2007-11-01" @default.
- W2374285163 modified "2023-09-24" @default.
- W2374285163 title "[Detecting perfluorooctanoic acid by reversed phase high performance liquid chromatography with pre-column ultraviolet derivatization]." @default.
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