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- W2374552125 abstract "A terephthalic acid-zinc complex(MOF-L) was prepared by solvothermal reaction using zinc nitrate and H2BDC as the reactants,N,N′-dimethylformamide(DMF) as the solvent.The properties of the resulting products have been characterized by using XRD,TG and low temperature nitrogen adsorption-desorption techniques.The results show that the pore size is bimodal distribution with sizes of ≤1 nm and 1.5～2.0 nm.On surface of MOF-L,there are two binding sites in the ultramicropore and supermicropore range,respectively.Wide pore size distribution leads to wide surface energy distribution and more energy peaks,as well as the type of adsorption site.When calcined at 300 ℃,the Langmuir specific surface area and total pore volume(Vp(N2,0.995)) is respectively 1243 m2·g-1 and 0.46 cm3· g-1.The hydrogen adsorption capability is 1.3wt% at 77 k and 1 bar.When the calcination temperature is at 400 ℃,the Langmuir specific surface area、total pore volume and hydrogen adsorption capability decline to 1 113 m2·g-1,0.43 cm3·g-1 and 0.8wt% respectively due to the collapse of the framework." @default.
- W2374552125 created "2016-06-24" @default.
- W2374552125 creator A5036621108 @default.
- W2374552125 date "2008-01-01" @default.
- W2374552125 modified "2023-09-25" @default.
- W2374552125 title "Porous Structure Analysis of Terephthalic Acid-Zinc Complex" @default.
- W2374552125 hasPublicationYear "2008" @default.
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