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- W2374554328 abstract "In the presence of ionic liquid [bmim][dca] as green reaction solvent and 4-[N,N′-dimethylamino-]pyridine(DMAP) as catalyst,β-cyclodextrin dehydroabietate(CDDA) was synthesized by the O-acylation reaction of dehydroabietic chloride with β-cyclodextrin.The optimum synthetic conditions of the target product were obtained as follows: molar ratio of dehydroabietic chloride to the hydroxyl group per D-glucose unit,3∶1;mass ratio of DMAP to dehydroabietic chloride,1∶20;reaction temperature,90 °C;and reaction time,1.5 h.The target product was analyzed and characterized by means of IR,XRD,SEM,TG-DTA,and elemental analysis.The property test results showed that compared with the raw β-cyclodextrin the target product's solubility,resistance to acids and bases,and hydrophobicity were well improved." @default.
- W2374554328 created "2016-06-24" @default.
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- W2374554328 date "2011-01-01" @default.
- W2374554328 modified "2023-09-23" @default.
- W2374554328 title "Study on Synthesis of β-Cyclodextrin Dehydroabietate in Ionic Liquid [bmim][dca]and Its Properties" @default.
- W2374554328 hasPublicationYear "2011" @default.
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