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- W2374556090 abstract "A highperformance liquid chromatographic tandem mass spectrometry(LC-MS) method was presented for determination of diaveridine in pig faeces and urine. The urine sample was treated with ethyl acetate. The organic phase was evaporated and redissolved with acetonitrile /water(35∶65); the faeces were extracted by ethyl acetate and purified with MCX solid phase extraction column, then the eluant was evaporated and redissolved with acetonitrile /water(35∶65).The result showed that the density of diaveridine in pig faeces and urine was in good linearity at the range of 5~1 000 μg/kg and 10~1 000 μg/L respectively(r0.99).The limit of quantification(LOQ) in urine and faeces were 10 μg/L and 5 μg/kg respectively. The recovery was 79.6%, 84.3%,90.2% while blank swine urine spiked with diaveridine at 10, 100, 1 000 μg/L and the recovery was 66.1%, 65.1%, 54.7% while blank swine faeces spiked with diaveridine at 10,100, 1 000 μg/kg respectively." @default.
- W2374556090 created "2016-06-24" @default.
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- W2374556090 date "2013-01-01" @default.
- W2374556090 modified "2023-09-28" @default.
- W2374556090 title "Determination of diaveridine in pig faeces and urine by high performance liquid chromatographic tandem mass spectrometry" @default.
- W2374556090 hasPublicationYear "2013" @default.
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