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- W2374821909 abstract "NH+4/molybdenum disulfide intercalated material was prepared by the exfoliation and restacking process.It could be used to store the single-layered molybdenum disulfide for a long time.It could be also used as a precursor to be inserted with other guest molecules to prepare new intercalated materials.The intercalated material was characterized by XRD and TGA.The results indicated that the interlayer spacing in the MoS2 was increased from 0.615 nm to 0.954 nm.The content of the inserted NH+4 was determined by elemental analysis and TGA,which showed that the as-prepared NH+4/molybdenum disulfides were(NH+4)3.1MoS2 and(NH+4)2.9MoS2 respectively.According to the results of XRD and TGA,no change of the intercalation compound was found after it had been saved in air for one month.The degree of intercalation was found to be dependent on the concentration of NH4Cl,the reaction temperature and time.The NH+4/molybdenum disulfide with the biggest interlayer spacing was obtained when the concentration of NH4Cl was 1.0%,reaction tempe-rature 30 ℃ and the reaction time 12 h." @default.
- W2374821909 created "2016-06-24" @default.
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- W2374821909 date "2008-01-01" @default.
- W2374821909 modified "2023-09-25" @default.
- W2374821909 title "Preparation and Characterization of Molybdenum Disulfide with NH_4~+ Interlayer" @default.
- W2374821909 hasPublicationYear "2008" @default.
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