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- W2374861384 abstract "A method preparing sulfaguanidine(SG)imprinted polymer microspheres by precipitation polymerization was developed,in which SG,methacrylic acid(MAA)and ethylene glycol dimethacrylate(EGDMA)were used as template molecule,functional monomer and crosslinker,respectively.The selectivity and adsorption properties of these microspheres were investigated.The optimized amounts of reactants were 0.05mmol SG,0.2mmol MAA,and 1mmol EGDMA(molar ratio 1∶4∶20).Under this condition, the volume of acetonitrile as solvent was 5mL and the amount of azobisisobutyronitrile(AIBN)as initiator was 10mg.The microspheres were polymerized at 60℃for 24h.The result of static equilibrium isotherm experiment revealed that molecularly imprinted polymer(MIP)had high bingding affinity and selectivity to sulfamidine.Scatchard analysis showed that there were two different kinds of binding sites in the MIP.The dissociation constant and the maximum adsorption capacity were 1.932mmol/L and 196.06μmol/g for the high affinity site,and they were 23.843mmol/L and 1 449.04μmol/g for the low affinity site,respectively. The MIP microspheres could be reused ten times without significant decrease on adsorption properties,as well used in solid phase extraction column as fillers.." @default.
- W2374861384 created "2016-06-24" @default.
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- W2374861384 date "2014-01-01" @default.
- W2374861384 modified "2023-09-23" @default.
- W2374861384 title "Synthese and Molecular Recognition Characteristics of Sulfaguanidine Imprinted Polymer Microspheres" @default.
- W2374861384 hasPublicationYear "2014" @default.
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