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- W2375113090 abstract "Objective: To establish an HPLC method for the simultaneous determination of berberine hydrochloride and linderane in Baiyao rectal solution. Methods: A ZORBAX SB- C18column( 250 mm × 4. 6 mm,5 μm) was used,and the mobile phase was acetonitrile( A)- 0. 1% phosphoric acid( B) and eluted with a gradient( 0- 5 min,40% A; 5- 10 min,40% A →60% A; 10- 15 min,60% A; 15- 20 min,60% A →40% A). The flow rate was1. 0 mL·min- 1,the detection wavelength was set at 235 nm,and the column temperature was maintained at 30 ℃.Results: The linear ranges of berberine hydrochloride and linderane were 21. 20- 212. 0 μg·mL- 1( r =0.9995)and 10. 72- 107. 2 μg·mL- 1( r =0.9997),respectively; the mean recoveries were 98. 8% and 98. 6% with RSDs of 1. 4% and 1. 6%,respectively. Conclusion: The established method is sensitive and specific,which can be used for quality control of Baiyao rectal solution." @default.
- W2375113090 created "2016-06-24" @default.
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- W2375113090 date "2014-01-01" @default.
- W2375113090 modified "2023-09-26" @default.
- W2375113090 title "HPLC simultaneous determination of berberine hydrochloride and linderane in Baiyao rectal solution" @default.
- W2375113090 hasPublicationYear "2014" @default.
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