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- W2375389873 abstract "OBJECTIVE To establish an HPLC-ELSD method for the determination of related substances in Glucosamine hydrochloride.METHODS The column of Zorbax SB-C18(250 mm×4.6 mm,5 μm)was used with a mobile phase consisted of 0.1% trifluoroacetic acid solution-acetonitrile(90:10)at a flow rate 0.8 ml·min-1.The temperature was 30℃.A Dikma Sedex 75 ELSD detector of drift tube temperature at 45℃ was used and the pressure of nebulizing gas was 3.5 bar.RESULTSThe peaks of glucosamine hydrochloride and specified from others impurity was well separated and the LOD was 40 ng.CONCLUSIONThe method is accurate,sensitive and rapid,which can be used for determination of the related substances in Glucosamine hydrochloride." @default.
- W2375389873 created "2016-06-24" @default.
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- W2375389873 date "2008-01-01" @default.
- W2375389873 modified "2023-09-22" @default.
- W2375389873 title "Determination of related substances in Glucosamine hydrochloride by HPLC-ELSD" @default.
- W2375389873 hasPublicationYear "2008" @default.
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