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- W2375453347 abstract "α-hydroxycyclohexylphenylketone is synthesized by one step using α-sulfocyclohexanecar boxylic acid as raw material.α-sulfocyclohexanecarboxylic acid,extracted from the by-product of sulphonation of producing hexanolactam with methylbenzene from 608 waste liquid provided by Baling Petrochemical Corp.Study on the experiment shows that α-sulfocyclohexanecarboxylic acid is extracted combining with the methods of coprecipitation reduction and complex extraction with the yield 85.7% and the purity 95%.One step reaction process: m(disodium α-sulfonatocyclohexanecarboxylate): m(benzoic acid)=2.2∶2.44,catalyst MnO,the reaction temperature 330 ℃,concentration of catalyst up to 0.99 wt%,reaction time 2 h,the yield of α-hydroxycyclohexylphenylketone 70.4%,purity 80.5%." @default.
- W2375453347 created "2016-06-24" @default.
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- W2375453347 date "2009-01-01" @default.
- W2375453347 modified "2023-09-26" @default.
- W2375453347 title "Study on synthesis of α-hydroxycyclohexylphenylketone in one step" @default.
- W2375453347 hasPublicationYear "2009" @default.
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