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- W2375589024 abstract "Silver sols were prepared from silver nitrate by chemical reduction in liquid phase,with ascorbic acid as the reducing agent and modified polyvinylpyrrolidone as the protecting agent.A nanometer silver powder with regular spherical shape was got from the sols treated with centrifugal-separating,washing and vacuum-drying.Effects of reaction temperature and solution pH value on particle size of the nano silver were studied using dynamic light scattering laser particle size analyzer.Features of the nano silver were observed by scanning electron microscopy,and crystal structure of the nano silver was characterized through X-ray diffraction.The results show that a nano silver powder with regular spherical shape and self-similar structure embedded in three-grade cycle at least can be obtained under the reaction conditions of 40 ℃,PVP/AgNO3=0.8,c(AgNO3)=0.24 mol/L,and pH value of ascorbic acid solution at 10.The nano-silver powder aggregate is pure and inclusion free,particle size of which is between 500 nm and 1 000 nm,and of the initially formed particle is 9～20 nm." @default.
- W2375589024 created "2016-06-24" @default.
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- W2375589024 date "2009-01-01" @default.
- W2375589024 modified "2023-09-28" @default.
- W2375589024 title "Preparation of Nano-Silver Powder with Self-Similar Structure" @default.
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