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- W2375626901 abstract "Poly-o-phenylenediamine modified glassy carbon electrode was successfully prepared by potentiostatic technique in phosphate buffer solution.It was found that the electrode had a significant electrocatalytic activity toward the reduction of H2O2.The poly-o-phenylenediamine membrane morphology was characterized using scanning electron microscopy.Various preparing conditions affecting the electrocatalytic activity of the membrane electrode were investigated and found that the membrane electrode prepared only in weak acidic conditions had higher electrocatalytic activity.The optimal film-forming potential,time and monomer concentration were 0.75 V,50 min,more than 6.0 mmol·L-1,respectively.The reaction on membrane electrode was controlled by adsorption at low scanning rate,demonstrating the electrochemical characteristics of thin-layers,and controlled by diffusion at high potential scanning rate,respectively.The linear regression equations toward the response to H2O2 were ΔIp(μA)=0.435+0.494cH2O2(mmol·L-1)(r=0.997 5,n=18) and ΔIp(μA)=9.36+0.894cH2O2(mmol·L-1) (r=0.999 4,n=15) in 5.88×10-2-23.5 mmol·L-1 and 25.3-48.4 mmol·L-1,respectively." @default.
- W2375626901 created "2016-06-24" @default.
- W2375626901 creator A5026347224 @default.
- W2375626901 date "2008-01-01" @default.
- W2375626901 modified "2023-10-16" @default.
- W2375626901 title "Establishment and Characterization of Poly-o-phenylenediamine Modified Glassy Carbon Electrode Prepared by Potentiostatic Technique" @default.
- W2375626901 hasPublicationYear "2008" @default.
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