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- W2376454016 abstract "Tetraethoxysilane(TEOS),methyl triethoxysilane(MTES) and caporlactam(CPL) were used to synthesize hydrophobic polyamide 6(PA6)/SiO2 hybrid material by in-situ and anionic ring-opening polymerization method.The outstretched Si-methyl groups on the surface of PA6/SiO2 hybrid material contribute to hydrophobicity.The contact angle θ on the surface of hybrid material is increasing with the increase of the content silica sol(SiO2% mass fraction)and keeps stable at about 130° for SiO2% 8.5.From the transform infrared spectroscopy(FT-IR) and X-ray photoelectron spectroscopy(XPS) spectra,the hydroxyl and ethoxyl groups of the silica sol drawn from partially hydrolysis and polycondensation between TEOS and MTES can react with PA6 precursor.Moreover,X-ray difftaction analysis(XRD) results show that the PA6 and the hydrophobic PA6/SiO2 hybrid materials synthesized in this paper are both of α crystal form,but from differential scanning calorimetry(DSC) curves,the melting point of PA6/SiO2 hybrid material is slightly higher than that of PA6." @default.
- W2376454016 created "2016-06-24" @default.
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- W2376454016 date "2008-01-01" @default.
- W2376454016 modified "2023-09-26" @default.
- W2376454016 title "Preparation and Characteristic of Hydrophobic Polyamide 6/SiO_2 Hybrid Material" @default.
- W2376454016 hasPublicationYear "2008" @default.
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