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- W2376740516 abstract "A new method for gravimetry of high content Ru in difficultly dissolved Ru-B solder using NaBH 4-H 2 reduction was established.The conditions were studied,systematically.The acerbity decomposition method of glass-envelop-tube for sample was compared with alkali fusing method,and at the same time,the gravimetry of NaBH 4-H 2 reduction for Ru was compared with distillation-thiourea color spectrophotometry.The results showed that the acerbity decomposition method of glass-envelop-tube was time-comsuming and its operation was much complex than the alkali fusing method,but the system of gravimetry was simple.The gravimetry of NaBH 4-H 2 reduction was time-comsuming than the distillation-thiourea color spectrophotometry,but because of high determining concentration of Ru,its relative error was less.For the determination of 50 mg~100 mg of Ru,relative error was-0.24%~+0.25%.The proposed method has high accuracy,good selectivity and better applicability,and it has been applied to determine Ru in Ru-B solder with satisfactory results." @default.
- W2376740516 created "2016-06-24" @default.
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- W2376740516 date "2009-01-01" @default.
- W2376740516 modified "2023-09-24" @default.
- W2376740516 title "Gravimetry for the Determination of Ru in Difficultly Dissolved Ru-B Solder Using NaBH_4-H_2 Reduction" @default.
- W2376740516 hasPublicationYear "2009" @default.
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