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- W2377037247 abstract "p-Nitroaniline is prepared by aminolysising of p-nitrochlorobenzene.The effects of reaction temperature,the concentration of ammonia solution,reaction time and the times of recycling the mother solution on the aminolysising process are investigated.The results show that,this process discharges less waste water but produces high-purity p-nitrochlorobenzene without the purification step.The conversion of p-nitrochlorobenzene and the purity of the formed p-nitroaniline can reach 100% and 99.9%,respectively,under the following conditions:31.5 g of p-nitrochlorobenzene,300.0 mL of 35% ammonia solution,170.0℃ of reaction temperature and 8.0 hours of reaction time.The yield of p-nitroaniline is 97.7%.The mother solution can be recycled for five times." @default.
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- W2377037247 date "2012-01-01" @default.
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- W2377037247 title "Research on production technology of p-nitroaniline with high purity" @default.
- W2377037247 hasPublicationYear "2012" @default.
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