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- W2377092334 abstract "OBJECTIVE To establish a method for determination residual acetonitrile,dichloromethane,tetrahydrofuran of Cefonicid Sodium by headspace GC.METHODS The GC was equipped with a flame-ionization detector for headspace injecting.A HP-INNOWAX(30m×0.53mm,1.0μm)chromatographic column was adopted.The carrier gas was nitrogen.Assay of residual solvents was calculated according to the external standard method.RESULTS Three residual solvents in Cefonicid sodium had good linear in the range of 6～600 μg·ml~ -1 (r≥0.9997).The average recovery was 98.7%～103.2%,with RSD 1.3%～1.8%.CONCLUSION The method is rapid,accurate and suitable for the determination of residual solvents in Cefonicid Sodium." @default.
- W2377092334 created "2016-06-24" @default.
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- W2377092334 date "2006-01-01" @default.
- W2377092334 modified "2023-09-23" @default.
- W2377092334 title "Detection method study of the residual solvents in Cefonicid Sodium" @default.
- W2377092334 hasPublicationYear "2006" @default.
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