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- W2377184219 abstract "2,6,2′,6′-Tetramethylazobenzene was synthesized from 2,6-xylidine using(C8～10H17~21)3N+CH3Cl-(A-1) as a phase transfer catalyst and K3Fe(CN)6 and NaOH as condensation agents.The optimal reaction conditions at 95 ℃ for 15 min from orthogonal experiment were as follows: 1 was 50 mmol,n[K3Fe(CN)6] ∶n(1)=5 ∶1,w(A-1) was 5%.The yield was 45.87% under the conditions." @default.
- W2377184219 created "2016-06-24" @default.
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- W2377184219 date "2007-01-01" @default.
- W2377184219 modified "2023-09-26" @default.
- W2377184219 title "Synthesis of 2,6,2′,6′-Tetramethylazobenzene by Phase Transfer Catalyst" @default.
- W2377184219 hasPublicationYear "2007" @default.
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