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- W2377758214 abstract "Two methods were used in synthesizing 1,4 Benzenediol monoacetate with the catalyst D001 resin. The result shows that a high conversion and a good selectivity can be achieved by using these two methods; The acetic anhydride is more active than acetic acid, so the reaction of acetic anhydride is easier than that of acetic acid. The suitable reaction conditions between 1,4 benzenediol and acetic anhydride in ethyl acetate are as follows: n(1,4 benzenediol)∶n(actic anhydride)=1∶1.2,the reaction temperature 80℃,the reaction time 1 h. This can result in a yield of 41.4% for 1,4 benzenediol monoacetate. The yield can reach 51.6% by reacting 1,4 benzenediol and acetic acid in toluene solution at refluxing temperature for 8 h." @default.
- W2377758214 created "2016-06-24" @default.
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- W2377758214 date "2001-01-01" @default.
- W2377758214 modified "2023-09-25" @default.
- W2377758214 title "Study on Synthesis of 1,4-Benzenediol Monoacetate" @default.
- W2377758214 hasPublicationYear "2001" @default.
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