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- W2378191678 abstract "Objective:To establish a quantified analytical method for determination of Cefradine in human plasma by HPLC-MSMS. Methods: The HPLC-MSMS conditions adopted were as follows: Symmetry ShieldTM Rp18(100 mm× 2.1 mm, 3.5 μm). The mobile phase consisted of acetonitrile-water (8∶92). The flow rate was 0.3 mL/min. Acyclovir was used as internal standard. Results: In human plasma, the standard curve was linear from 0.1～30.0 μg/mL, A = 1.3 - 0.008 63(r = 0.997 0, n = 8). The lower limit of quantification of cefradine was 0.1 μg/mL. The RSD of within-day was less than 3.90%, the RSD of between-day was less than 14.90%, and the method recovery rate was 107.60%～108.70%. Conclusion: The assay was simple to operate, accurate, reliable and time-saving short analysis time. It is suitable for the clinical pharmacokinetics and bioequivalence studies." @default.
- W2378191678 created "2016-06-24" @default.
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- W2378191678 date "2009-01-01" @default.
- W2378191678 modified "2023-09-25" @default.
- W2378191678 title "Determination of Cefradine in Human Plasma by LC-MS/MS Method" @default.
- W2378191678 hasPublicationYear "2009" @default.
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