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- W2378625420 abstract "A high performance liquid chromatography with solid-phase extraction method was developed for the determination of benzo(a)pyrene in meat products.The extracted sample was purified on a Cleanert BaP solid-phase extraction column and separated on a Waters SunFire C18 column(4.6 mm × 250 mm,5μm) using a mobile phase composed of acetonitrile and water(88/12) at a flow rate of 1.0 mL/min.Benzo(a)pyrene was measured using a fluorescence detector at an excitation wavelength of 386 nm and an emission wavelength of 405 nm.The result showed that benzo(a)pyrene displayed good linearity relationship over the concentration range of 0.5-10 ng/mL,with a coefficient correlation of 0.9978.The limit of detection was 0.04 μg/kg,and the precision(RSD) for 6 replication determinations was below 5%.The average blank spike recoveries across the levels was in the range of 82.2%-94.9%(n=3).This method was rapid,simple,reproducible,and applicable for benzo(a)pyrene determination in meat products,providing guarantee for quality control and safety evaluation of meat products." @default.
- W2378625420 created "2016-06-24" @default.
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- W2378625420 date "2012-01-01" @default.
- W2378625420 modified "2023-09-24" @default.
- W2378625420 title "Determination of Benzo(a)pyrene in Meat Products by HPLC with Solid-Phase Extraction" @default.
- W2378625420 hasPublicationYear "2012" @default.
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