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- W2378700749 abstract "The multi-shaped NiB nano /micro powders were prepared by chemical reduction method using sodium borohydride as reductant in several microemulsion systems comprised of different content of cetyl-trimethylammonium bromide(CTAB) n-amylalcohol and water.The phase composition and morphologies of the product samples obtained under different conditions were characterized by X-ray powder differaction,selected area electron diffraction and transmission electron microscope.The effect of reaction conditions such as the types of NiB,temperatures and concentrations of NaBH 4 on the hydrogen generation by hydrolysis of NaBH 4 were investigated in detail.The results show that the amorphous alloy NiB with high purity can be obtained by means of the microemulsion systems.With the increase of water concentration,the particle changes from sphere to dendritic shape and the average diameter of the NiB particles reduces with the increase of n-amylalcohol concentration.The as-prepared NiB in microemulsion system exhibits more activity than the regular NiB prepared in aqueous solution for the hydrolysis of NaBH 4.The less effect of NaBH 4 concentration in solution on hydrogen production rate endows the hydrolysis reaction with kinetic characteristics of zero-order reaction." @default.
- W2378700749 created "2016-06-24" @default.
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- W2378700749 date "2013-01-01" @default.
- W2378700749 modified "2023-09-28" @default.
- W2378700749 title "Hydrogen Generation by Hydrolysis of NaBH_4 Solution Using NiB Catalysts Prepared in Microemulsion Systems" @default.
- W2378700749 hasPublicationYear "2013" @default.
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