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- W2379113137 abstract "Dimethyl azobisisobutyrate was prepared by the reaction of hydrazobisiobutyronitrile,chlorine and methanol in presence of methanol as solvent.The optimum conditions for the synthesis of dimethyl azobisisobutyrate were determined: the molar ration of n(AIBN):n(chlorine):n(hydrochloride)=1:1.3:0.8,reaction temperature 20~25℃,and reaction time 18h.The yield was 93.6%,and the content was 99.3%.The product was assignd by IR and 1HNMR." @default.
- W2379113137 created "2016-06-24" @default.
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- W2379113137 date "2011-01-01" @default.
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- W2379113137 title "The Synthesis of Dimethyl Azobisisobutyrate" @default.
- W2379113137 hasPublicationYear "2011" @default.
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