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- W2379268858 abstract "A method of high performance liquid chromatography combined with gel permeation chromatography(GPC/HPLC) was developed for the simultaneous analysis of methyltestosterone(MET)and diethylstilbestrol(DES) in aquatic products.The homogenized samples were extracted with diethyl ether,then cleaned by GPC using ethyl acetate-cyclohexane(1 ∶ 1)as mobile phase,follwed by a further HLB solid phase extraction.The targeted compounds were detected by HPLC-ultraviolet detector at the wavelength of 254 nm,using methanol-water(72 ∶ 28) as mobile phase,and quantified by the external standard method.The calibration curves of two compounds were linear in the concentration range of 0.02-2.0 mg/L with correlation coefficients more than 0.999.The average recoveries of MET and DES at spiked concentrations of 10.0,50.0,200 μg/kg ranged from 84% to 93%,with relative standard deviations(RSDs) less than 6.0%.The LOQs of MET and DES were 6.0 μg/kg and 5.0 μg/kg,respectively." @default.
- W2379268858 created "2016-06-24" @default.
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- W2379268858 date "2013-01-01" @default.
- W2379268858 modified "2023-09-22" @default.
- W2379268858 title "Simultaneous Determination of Methyltestosterone and Diethylstilbestrol in Aquatic Products by Gel Permeation Chromatography-High Performance Liquid Chromatography" @default.
- W2379268858 hasPublicationYear "2013" @default.
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