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- W2379636732 abstract "Monovinyl-functionalized silsesquioxane cage,1,3,5,7,9,11,13-heptacyclopentyl-15-vinyl silsesquioxane(VinylPOSS),was prepared via the corner capping reaction of incompletely condensed silsesquioxanes,(C5H9)7Si7O9(OH)3,with vinyltrichlorosilane.VinylPOSS was characterized by FTIR,1H NMR,29Si NMR,13C NMR,elemental analysis,WAXD and TGA.The yield of VinylPOSS increased with reaction time,when vinyltrichlorosilane reacted with(C5H9)7Si7O9(OH)3 for 10 h,the yield was 90%.VinylPOSS has good solubility in weak polar solvent,and it shows good thermal stability,its temperature with 5% decomposition is 283℃ and the temperature with 56% residue is 800℃.The reactivity of VinylPOSS with high hydrogen-containing silicone fluid(HHSF) was investigated.It can be reacted with HHSF by Michael additions at both α-and β-positions,and the reaction is mainly β-addition." @default.
- W2379636732 created "2016-06-24" @default.
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- W2379636732 date "2009-01-01" @default.
- W2379636732 modified "2023-09-25" @default.
- W2379636732 title "Synthesis and characterization of monovinyl-functionalized silsesquioxane cage" @default.
- W2379636732 hasPublicationYear "2009" @default.
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