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- W2380069061 abstract "A novel 1D chainlike heteropoly compound,[DETA]4NaH2{Na[Mo6O12(OH)3(HPO4)(H2PO4)3]2}·8H2O(DETA= diethylenetriamine),which is constructed from sandwich-type polyanion {Na[Mo6O12(OH)3(HPO4)(H2PO4)3]2]3-has been hydrothermally synthesized and characterized by elemental analysis,IR,UV spectrum,TG analysis and single crystal X-ray diffraction analysis.The title compound crystallizes in the triclinic system,space group P-ī,a=12.421 2(4) nm,b=12.591 1(4) nm,c=13.078 2(4) nm,α=85.411 0(10)°,β=73.313 0(10)°,γ=82.276 0(10)°,V=1 939.63(11) nm3,Z=2,R1= 0.024 4.In the sandwich-type polyanion,Na atom interconnects two building blocks [Mo6O12(OH)3(HPO4)(H2PO4)3}2-via the bridging oxo groups,and adjacent polyanions are linked by another Na+ leading to the formation of a 1D sandwich-type chain structure.Each chain is further linked to two adjacent chains by hydrogen bonds to yield a 3D framework.The six MoO6 octahedra in the [Mo6O12(OH)3(HPO4)(H2PO4)3]2-cluster construct a Mo6 ring by sharing edges.The four PO4 tetrahedra are located at one face of the Mo6 ring." @default.
- W2380069061 created "2016-06-24" @default.
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- W2380069061 date "2009-01-01" @default.
- W2380069061 modified "2023-09-22" @default.
- W2380069061 title "Hydrothermal Synthesis and Structure of 1D Chainlike Heteropoly Compound" @default.
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