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- W2380201152 abstract "Objective To establish the method for qualitative identification and quantitative analysis of pyrrolidine dithiocarbamate(PDTC),a novel anti-tuberculosis agent.Methods PDTC was identified by chemical,ultraviolet(UV) and infrared(IR) spectroscopic methods and high-performance liquid chromatography(HPLC) combined with referrence control.A validated HPLC-UV method was used to determine the content of PDTC synthetic products.Results Chemical tests showed the characteristics of sulfur substituted chromogenic reactions.PDTC in 50% methanol had maximum absorption peaks at 255 nm and 278 nm wavelength.The VSHbroad-peak was strong in the 3 250,2 500 cm-1and the VCc=s Sbroad-peak was weak at 1 716 cm-1.PDTC synthetic product was determined,with the reference substance as control and the linear range of PDTC was 25.75-206.00 μg/mL(r = 0.999 8).The average recoveries at low, middle and high levels were 100.09%(RSD = 0.59%,n = 3),100.06%(RSD = 1.47%,n = 3),100.10%(RSD=0.58%,n= 3),respectively.Conclution The qualitative and quantitative methods are accurate, reliable and reproducible and could be used for the quality control of PDTC synthetic products." @default.
- W2380201152 created "2016-06-24" @default.
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- W2380201152 date "2014-01-01" @default.
- W2380201152 modified "2023-09-25" @default.
- W2380201152 title "Study on qualitative identification and quantitative analysis of pyrrolidine dithiocarbamate" @default.
- W2380201152 hasPublicationYear "2014" @default.
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