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- W2380328449 abstract "Objective To establish the hydride generation-atomic fluorescence spectrometric method for the determination of tin in human blood and urine with high-pressure microwave digestion and complexing ligand.Methods Human blood and urine samples were digested by using high-pressure microwave.Then complexing ligand 1% EDTA,5 ml 150 g/L thiourea and ascorbic acid were added to mask the interfering ions such as nickel,iron,arsenic,selenium and etc.Tin concentration was determined with hydride-generation atomic fluorescence spectrometric method with sodium borohydride as the reductant in 2% sulphuric acid media.Results The linear range of tin was 10-100 μg/ml,the regression equations and correlation coefficients in blood and urine were y=9.391 1 x-16.312,r=0.999 7,y=8.244 7x-27.849 6,r=0.998 2,respectively.The limits of detection of tin in blood and urine were 0.090,0.020 μg/L respectively.The relative standard derivation of this method was 1.4%-6.1%.The rates of recovery were between 98.1% and 101.8%.Conclusion This method presents many advantages,such as completed sample digestion,rapid,less matrix disturbance,accurate,sensitive and is applicable to the determination of tin in blood and urine in grass-roots units." @default.
- W2380328449 created "2016-06-24" @default.
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- W2380328449 date "2013-01-01" @default.
- W2380328449 modified "2023-09-28" @default.
- W2380328449 title "Determination of tin in human blood and urine with high-pressure microwave digestion and complexing ligand and hydride generation-atomic fluorescence spectrometry" @default.
- W2380328449 hasPublicationYear "2013" @default.
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