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- W2380397149 abstract "A gas chromatography-mass spectro metry method(GC-MS)under selective ion monitoring mode was established for the simultaneous determination of six phthalates in canned food.Phthalates,namely,dibutyl phthalate(DBP), benzyl-n-butyl phthalate(BBP),di-(2-ethylhexyl)phthalate(DEHP),di-n-octyl phthalate(DNOP),diisononyl phthalate(DINP) and diisodecyl phthalate(DIDP)were extracted from samples with n-hexane and the extract was cleaned up by dispersive method with primary-secondary amine(PSA)sorbent.Good linear and lower limits of detection were obtained,the linears were between 0.1～5.0μg/mL(DBP,BBP,DEHP,DNOP),0.5～25.0μg/mL(DINP,DIDP),correlation coefficients were larger than 0.995,and the detection limits(S/N=10)were 0.01 mg/kg(DBP,BBP,DEHP,DNOP),1.0mg/kg(DINP,DIDP).Six common representative samples were selected to validate the method by recovery and precision.On the spike level of 0.2～2.0mg/kg(DBP,BBP,DEHP,DNOP),1.0～10.0 mg/kg(DINP,DIDP),the obtained recoveries were in the range of 80～130%,with RSDs less than 10%." @default.
- W2380397149 created "2016-06-24" @default.
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- W2380397149 date "2008-01-01" @default.
- W2380397149 modified "2023-09-23" @default.
- W2380397149 title "DETERMINATION OF SIX PHTHALATES IN CANNED FOOD BY GC-MS WITH DISPERSIVE SOLID-PHASE EXTRACTION" @default.
- W2380397149 hasPublicationYear "2008" @default.
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