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- W2380451634 abstract "Objective:To establish a quality control method for Xiaolei Mixture.Methods:The two main ingredients of Radix Astragali and Radix Scutellariae were identified by silical gel G thin layer chromatography and the baicalin was determined by RP-HPLC with a Zorbax Extend-C18(5 μm,4.6 mm×150 mm)column.The mobile phase was methanol–water-phosphoric acid(55∶45∶0.2).The flow rate was 1.0 mL·min-1.The detection wavelength was 280 nm.Results: The calibration curve was linear in the range of 13.44-134.4 μg·mL-1 for baicalin with r=0.9996.Within-day and between-day RSDs were 1.3% and 1.6%(n=3).The average recoveries of high,middle and low three concentrations from sample were 100.9%, 101.8%,102.2% with RSD=1.5%, 1.7%, 1.4%(n=3).Conclusions:The methods are simple, accurate and reliable, and can be used for the quality control of the Xiaolei Mixture" @default.
- W2380451634 created "2016-06-24" @default.
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- W2380451634 date "2010-01-01" @default.
- W2380451634 modified "2023-09-25" @default.
- W2380451634 title "Studies on the quality control method of Xiaolei Mixture" @default.
- W2380451634 hasPublicationYear "2010" @default.
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