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- W2380551431 abstract "Methyl monochloroacetate was prepared through continuous esternization method with mother liquor of chloroacetic acid and methanol as raw material and immobilized phosphotungstic acid as catalyst. With the yield of methyl monochloroacetate as evaluating standard,the synthesized condition of methyl chloroacetate was optimized through orthogonal experiment. The experimental results indicated the mass quantity ratio of the mother liquor to methanol or to catalyst had great influence on the yield of methyl monochloroacetate. The optimum condition as follows:the of mass quantity ratio of the mother liquor to methanol and catalyst was 10/7 and 10/1 respectively,the reflux time was 1.0 h. The yield of methyl monochloroacetate was 46.9% under these condition." @default.
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- W2380551431 date "2006-01-01" @default.
- W2380551431 modified "2023-09-26" @default.
- W2380551431 title "Optimization of Synthesized Condition of Methyl Chloroacetate through Mother Liquor of Chloroacetic Acid with Immobilized phosphotungstic Acid as Catalyst" @default.
- W2380551431 hasPublicationYear "2006" @default.
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