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- W2380769138 abstract "Balofloxacin was synthesized from ethyl 1-cyclopropyl-6,7-difluoro-1,4-dihydro-8-methoxy-4-oxoquinoline-3-carboxylate after boron chelation followed by condensation with 3-methylaminopiperidine and thenhydrolysis with an overall yield of 74.4%. The key intermediate 3-methylaminopiperidine was synthesized in 11.5% overallyield from g-butyrolactone via aminolysis, hydrolysis, esterification, condensation with ethyl bromoacetate, cyclization,decarboxylation, reductive amination and debenzylation." @default.
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- W2380769138 date "2004-01-01" @default.
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- W2380769138 title "Synthesis of Balofloxacin" @default.
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