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- W2382151207 abstract "Objective To seek the conditions of refinement of gentiopicroside from Gentiana macrophylla Pall.with macroporous resin. Methods Orthogonal design was used to select test faction,and the yield and the content of gentiopicroside were taken as indices to compare the purification effect in different technical parameters. Results That saturation ratio was 22.7mg/g(wet resin),and that absorption ratio was 20.5mg/g(wet resin).Then after L9(34) orthogonal trials and validation,when eluent was 40% ethanol,the ratio of gentiopicroside to macroporous resin was 12mg/g and the concentration of liquor was 18.5mg/ml,the yield and content of gentiopicroside in the sample were over 91% and 75%,respectively. Conclusion ADS-7 macroporous resin can successfully refine gentiopicroside,and the technical parameters can be referred by the scale-up trials." @default.
- W2382151207 created "2016-06-24" @default.
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- W2382151207 date "2012-01-01" @default.
- W2382151207 modified "2023-09-23" @default.
- W2382151207 title "Optimization of Purification of Gentiopicroside from Gentiana macrophylla by Orthogonal Test" @default.
- W2382151207 hasPublicationYear "2012" @default.
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