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- W2382314696 abstract "The title complex is synthesized and characterized by Xray diffraction at 293(2) K. In the complex, the ligand exists in monopro tonated form with its one proton attached to the imine group.it functions as a b ridge ligand and coordinates with its two monodentate acetate oxygen atoms to tw o manganese(Ⅱ) ions. Each Mn(Ⅱ) is surrounded by four monodentate acetate grou ps from four independent iminodiacetate ligands ［Mn(Ⅱ)-O(carboxy)=0.217 3(2) n m］ and two additional ligands, i.e.,water molecules ［Mn(Ⅱ)-O(aqua)=0.212 9(2) nm］, are coordinated at the axial positions, resulting in a distorted octahed ral geometry as well as layer structure. Between twodimensional layers there are rich hydrogen bonds, which exist among the uncoordinated carboxyl oxygen atoms, the aqua ligands and the protonated nitrogen atoms, therefore, the complex forms into a threedimensional network.The crystal is in a tetragonal system, space group p421c, with a=0.805 70(1) nm, c=0.955 1(3) nm, V=0.620 0(2) nm3, Z=2, Mr=355.17, and Dc=1.902 mg/m 3, F(000)=366, μ=1.125 mm-1. For 465 independent reflections ［I2σ(I)］,the final R factor is 0.019 6, and Rw is 0.0553" @default.
- W2382314696 created "2016-06-24" @default.
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- W2382314696 date "2000-01-01" @default.
- W2382314696 modified "2023-09-25" @default.
- W2382314696 title "Crystal structure of bis(Nprotonate d iminodiacetato)manganese(II)" @default.
- W2382314696 hasPublicationYear "2000" @default.
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