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- W2382677682 abstract "Objective: To improve the synthetic process of prasugrel hydrochloride. Methods: The target compound was synthesized from 5,6,7,7a-tetrahydro-thieno[3,2-c]pyridin-2-( 4H)-one hydrochloride and 2-bromo-1-cyclopropyl-2-( 2-fluorophenyl) ethanone as the starting materials via three steps including substitution,acylation and salification. Results: The structure of the target compound was confirmed by MS,1H-NMR and IR. The total yield was 60%,and the HPLC purity was more than 99. 5%. Conclusion: The improved process with simplified operation and good yield is applicable to pilot manufacture." @default.
- W2382677682 created "2016-06-24" @default.
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- W2382677682 date "2014-01-01" @default.
- W2382677682 modified "2023-09-25" @default.
- W2382677682 title "An improved process for synthesis of prasugrel hydrochloride" @default.
- W2382677682 hasPublicationYear "2014" @default.
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